Separation of mono- and bis-phosphonium salts by preparative HPLC

P. Jandik; U. Deschler; H. Schmidbaur

doi:10.1007/BF00483195

Separation of mono- and bis-phosphonium salts by preparative HPLC

P. Jandik
, U. Deschler
, H. Schmidbaur

Department of Chemistry

Technical University of Munich

Research output: Contribution to journal › Article › peer-review

4 Scopus citations

Abstract

Development and application of a preparative HPLC method for the separation of phosphonium salts is described. Analytical chromatograms obtained by means of ion-pair chromatography as well as adsorption chromatography in the presence or absence of acid are presented. A description of successful preparative separations is also given. The chromatographic fractions were identified by ¹H- and ³¹P-NMR spectroscopy.

Original language	English
Pages (from-to)	347-354
Number of pages	8
Journal	Fresenius Zeitschrift fur Analytische Chemie
Volume	305
Issue number	5
DOIs	https://doi.org/10.1007/BF00483195
State	Published - Jan 1981

Keywords

Chromatographie, HPLC
NMR-Spektroskopie
Trenn. von Phosphoniumsalzen

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10.1007/BF00483195

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title = "Separation of mono- and bis-phosphonium salts by preparative HPLC",

abstract = "Development and application of a preparative HPLC method for the separation of phosphonium salts is described. Analytical chromatograms obtained by means of ion-pair chromatography as well as adsorption chromatography in the presence or absence of acid are presented. A description of successful preparative separations is also given. The chromatographic fractions were identified by 1H- and 31P-NMR spectroscopy.",

keywords = "Chromatographie, HPLC, NMR-Spektroskopie, Trenn. von Phosphoniumsalzen",

author = "P. Jandik and U. Deschler and H. Schmidbaur",

year = "1981",

month = jan,

doi = "10.1007/BF00483195",

language = "English",

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journal = "Fresenius Zeitschrift fur Analytische Chemie",

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T1 - Separation of mono- and bis-phosphonium salts by preparative HPLC

AU - Jandik, P.

AU - Deschler, U.

AU - Schmidbaur, H.

PY - 1981/1

Y1 - 1981/1

N2 - Development and application of a preparative HPLC method for the separation of phosphonium salts is described. Analytical chromatograms obtained by means of ion-pair chromatography as well as adsorption chromatography in the presence or absence of acid are presented. A description of successful preparative separations is also given. The chromatographic fractions were identified by 1H- and 31P-NMR spectroscopy.

AB - Development and application of a preparative HPLC method for the separation of phosphonium salts is described. Analytical chromatograms obtained by means of ion-pair chromatography as well as adsorption chromatography in the presence or absence of acid are presented. A description of successful preparative separations is also given. The chromatographic fractions were identified by 1H- and 31P-NMR spectroscopy.

KW - Chromatographie, HPLC

KW - NMR-Spektroskopie

KW - Trenn. von Phosphoniumsalzen

UR - https://www.scopus.com/pages/publications/0004597614

U2 - 10.1007/BF00483195

DO - 10.1007/BF00483195

M3 - Article

AN - SCOPUS:0004597614

SN - 0016-1152

VL - 305

SP - 347

EP - 354

JO - Fresenius Zeitschrift fur Analytische Chemie

JF - Fresenius Zeitschrift fur Analytische Chemie

IS - 5

ER -

Separation of mono- and bis-phosphonium salts by preparative HPLC

Abstract

Keywords

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