Separation of mono- and bis-phosphonium salts by preparative HPLC

P. Jandik; U. Deschler; H. Schmidbaur

doi:10.1007/BF00483195

Separation of mono- and bis-phosphonium salts by preparative HPLC

P. Jandik, U. Deschler, H. Schmidbaur

Department of Chemistry

Technical University of Munich

Research output: Contribution to journal › Article › peer-review

4 Scopus citations

Abstract

Development and application of a preparative HPLC method for the separation of phosphonium salts is described. Analytical chromatograms obtained by means of ion-pair chromatography as well as adsorption chromatography in the presence or absence of acid are presented. A description of successful preparative separations is also given. The chromatographic fractions were identified by ¹H- and ³¹P-NMR spectroscopy.

Original language	English
Pages (from-to)	347-354
Number of pages	8
Journal	Fresenius' Zeitschrift für Analytische Chemie
Volume	305
Issue number	5
DOIs	https://doi.org/10.1007/BF00483195
State	Published - Jan 1981

Keywords

Chromatographie, HPLC
NMR-Spektroskopie
Trenn. von Phosphoniumsalzen

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10.1007/BF00483195

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abstract = "Development and application of a preparative HPLC method for the separation of phosphonium salts is described. Analytical chromatograms obtained by means of ion-pair chromatography as well as adsorption chromatography in the presence or absence of acid are presented. A description of successful preparative separations is also given. The chromatographic fractions were identified by 1H- and 31P-NMR spectroscopy.",

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author = "P. Jandik and U. Deschler and H. Schmidbaur",

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AU - Deschler, U.

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N2 - Development and application of a preparative HPLC method for the separation of phosphonium salts is described. Analytical chromatograms obtained by means of ion-pair chromatography as well as adsorption chromatography in the presence or absence of acid are presented. A description of successful preparative separations is also given. The chromatographic fractions were identified by 1H- and 31P-NMR spectroscopy.

AB - Development and application of a preparative HPLC method for the separation of phosphonium salts is described. Analytical chromatograms obtained by means of ion-pair chromatography as well as adsorption chromatography in the presence or absence of acid are presented. A description of successful preparative separations is also given. The chromatographic fractions were identified by 1H- and 31P-NMR spectroscopy.

KW - Chromatographie, HPLC

KW - NMR-Spektroskopie

KW - Trenn. von Phosphoniumsalzen

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JF - Fresenius' Zeitschrift für Analytische Chemie

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ER -

Separation of mono- and bis-phosphonium salts by preparative HPLC

Abstract

Keywords

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