Redetermination of the crystal structure of di-(4,7,13,16,21,24-hexaoxa- 1,10-diazabicyclo[8.8.8]hexacosane-κ8N2,O6) potassium - Tetrapotassium octadecagermanide - Ethylenediamine (1:1:7), C25H64Ge9K3N9O6

Kerstin Mayer; Michael Giebel; Manuel M. Bentlohner; Wilhelm Klein; Thomas F. Fässler

doi:10.1515/ncrs-2015-0020

Redetermination of the crystal structure of di-(4,7,13,16,21,24-hexaoxa- 1,10-diazabicyclo[8.8.8]hexacosane-κ⁸N₂,O₆) potassium - Tetrapotassium octadecagermanide - Ethylenediamine (1:1:7), C₂₅H₆₄Ge₉K₃N₉O₆

Kerstin Mayer, Michael Giebel, Manuel M. Bentlohner, Wilhelm Klein, Thomas F. Fässler

Chair of Inorganic Chemistry with Focus on New Materials

Technical University of Munich

Research output: Contribution to journal › Article › peer-review

6 Scopus citations

Abstract

C₂₅H₆₄Ge₉K₃N₉O₆, triclinic, P1 (no. 2), a = 9.3766(7) A, b = 13.540(1) A, c = 19.507(1) A, α = 84.527(3)°, β = 81.252(3)°, γ = 80.127(4)°, V = 2405.4 A³, Z = 2, R_gt(F) = 0.0405, wR_ref(F²) = 0.1050, T = 123 K.

Original language	English
Pages (from-to)	286-288
Number of pages	3
Journal	Zeitschrift fur Kristallographie - New Crystal Structures
Volume	230
Issue number	3
DOIs	https://doi.org/10.1515/ncrs-2015-0020
State	Published - 1 Sep 2015

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Mayer, K., Giebel, M., Bentlohner, M. M., Klein, W., & Fässler, T. F. (2015). Redetermination of the crystal structure of di-(4,7,13,16,21,24-hexaoxa- 1,10-diazabicyclo[8.8.8]hexacosane-κ⁸N₂,O₆) potassium - Tetrapotassium octadecagermanide - Ethylenediamine (1:1:7), C₂₅H₆₄Ge₉K₃N₉O₆. Zeitschrift fur Kristallographie - New Crystal Structures, 230(3), 286-288. https://doi.org/10.1515/ncrs-2015-0020

Mayer, Kerstin ; Giebel, Michael ; Bentlohner, Manuel M. et al. / Redetermination of the crystal structure of di-(4,7,13,16,21,24-hexaoxa- 1,10-diazabicyclo[8.8.8]hexacosane-κ⁸N₂,O₆) potassium - Tetrapotassium octadecagermanide - Ethylenediamine (1:1:7), C₂₅H₆₄Ge₉K₃N₉O₆. In: Zeitschrift fur Kristallographie - New Crystal Structures. 2015 ; Vol. 230, No. 3. pp. 286-288.

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title = "Redetermination of the crystal structure of di-(4,7,13,16,21,24-hexaoxa- 1,10-diazabicyclo[8.8.8]hexacosane-κ8N2,O6) potassium - Tetrapotassium octadecagermanide - Ethylenediamine (1:1:7), C25H64Ge9K3N9O6",

abstract = "C25H64Ge9K3N9O6, triclinic, P1 (no. 2), a = 9.3766(7) A, b = 13.540(1) A, c = 19.507(1) A, α = 84.527(3)°, β = 81.252(3)°, γ = 80.127(4)°, V = 2405.4 A3, Z = 2, Rgt(F) = 0.0405, wRref(F2) = 0.1050, T = 123 K.",

author = "Kerstin Mayer and Michael Giebel and Bentlohner, {Manuel M.} and Wilhelm Klein and F{\"a}ssler, {Thomas F.}",

note = "Publisher Copyright: {\textcopyright} 2015 Walter de Gruyter GmbH, Berlin/Munich/Boston.",

year = "2015",

month = sep,

day = "1",

doi = "10.1515/ncrs-2015-0020",

language = "English",

volume = "230",

pages = "286--288",

journal = "Zeitschrift fur Kristallographie - New Crystal Structures",

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number = "3",

}

Mayer, K, Giebel, M, Bentlohner, MM, Klein, W & Fässler, TF 2015, 'Redetermination of the crystal structure of di-(4,7,13,16,21,24-hexaoxa- 1,10-diazabicyclo[8.8.8]hexacosane-κ⁸N₂,O₆) potassium - Tetrapotassium octadecagermanide - Ethylenediamine (1:1:7), C₂₅H₆₄Ge₉K₃N₉O₆', Zeitschrift fur Kristallographie - New Crystal Structures, vol. 230, no. 3, pp. 286-288. https://doi.org/10.1515/ncrs-2015-0020

Redetermination of the crystal structure of di-(4,7,13,16,21,24-hexaoxa- 1,10-diazabicyclo[8.8.8]hexacosane-κ⁸N₂,O₆) potassium - Tetrapotassium octadecagermanide - Ethylenediamine (1:1:7), C₂₅H₆₄Ge₉K₃N₉O₆. / Mayer, Kerstin; Giebel, Michael; Bentlohner, Manuel M. et al.
In: Zeitschrift fur Kristallographie - New Crystal Structures, Vol. 230, No. 3, 01.09.2015, p. 286-288.

Research output: Contribution to journal › Article › peer-review

TY - JOUR

T1 - Redetermination of the crystal structure of di-(4,7,13,16,21,24-hexaoxa- 1,10-diazabicyclo[8.8.8]hexacosane-κ8N2,O6) potassium - Tetrapotassium octadecagermanide - Ethylenediamine (1:1:7), C25H64Ge9K3N9O6

AU - Mayer, Kerstin

AU - Giebel, Michael

AU - Bentlohner, Manuel M.

AU - Klein, Wilhelm

AU - Fässler, Thomas F.

PY - 2015/9/1

Y1 - 2015/9/1

N2 - C25H64Ge9K3N9O6, triclinic, P1 (no. 2), a = 9.3766(7) A, b = 13.540(1) A, c = 19.507(1) A, α = 84.527(3)°, β = 81.252(3)°, γ = 80.127(4)°, V = 2405.4 A3, Z = 2, Rgt(F) = 0.0405, wRref(F2) = 0.1050, T = 123 K.

AB - C25H64Ge9K3N9O6, triclinic, P1 (no. 2), a = 9.3766(7) A, b = 13.540(1) A, c = 19.507(1) A, α = 84.527(3)°, β = 81.252(3)°, γ = 80.127(4)°, V = 2405.4 A3, Z = 2, Rgt(F) = 0.0405, wRref(F2) = 0.1050, T = 123 K.

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U2 - 10.1515/ncrs-2015-0020

DO - 10.1515/ncrs-2015-0020

M3 - Article

AN - SCOPUS:84942101873

SN - 1433-7266

VL - 230

SP - 286

EP - 288

JO - Zeitschrift fur Kristallographie - New Crystal Structures

JF - Zeitschrift fur Kristallographie - New Crystal Structures

IS - 3

ER -

Mayer K, Giebel M, Bentlohner MM, Klein W, Fässler TF. Redetermination of the crystal structure of di-(4,7,13,16,21,24-hexaoxa- 1,10-diazabicyclo[8.8.8]hexacosane-κ⁸N₂,O₆) potassium - Tetrapotassium octadecagermanide - Ethylenediamine (1:1:7), C₂₅H₆₄Ge₉K₃N₉O₆. Zeitschrift fur Kristallographie - New Crystal Structures. 2015 Sep 1;230(3):286-288. doi: 10.1515/ncrs-2015-0020