Quality criteria of the isotope dilution method for the determination of polycyclic aromatic hydrocarbons, petroleum-derived hydrocarbons and phenol in leachate of large-scale lysimeter experiments

Karl Werner Schramm; Bernhard Henkelmann; Daniela Peschke; Dieter Martens

doi:10.1007/s00769-005-0928-0

Quality criteria of the isotope dilution method for the determination of polycyclic aromatic hydrocarbons, petroleum-derived hydrocarbons and phenol in leachate of large-scale lysimeter experiments

Karl Werner Schramm, Bernhard Henkelmann, Daniela Peschke, Dieter Martens

Research output: Contribution to journal › Article › peer-review

Abstract

A comprehensive analytical procedure for polycyclic aromatic hydrocarbons, petroleum-derived hydrocarbons and phenol using the isotope dilution method and employing high-resolution gas chromatography and mass spectrometry was developed and validated for leachates from source-term experiments and the different sampling sites of lysimeters. The use of glassware and other materials is efficiently limited to minimize the risk of contamination. The relative standard deviation elaborated allows precise reliable measurements. Limit of detection and recovery data are useful to judge the quality of each single measurement.

Original language	English
Pages (from-to)	229-234
Number of pages	6
Journal	Accreditation and Quality Assurance
Volume	10
Issue number	5
DOIs	https://doi.org/10.1007/s00769-005-0928-0
State	Published - May 2005
Externally published	Yes

Keywords

High-resolution gas chromatography-mass spectrometry
Leachate
Lysimeter
Petroleum-derived hydrocarbons
Phenol
Polycyclic aromatic hydrocarbons
Validation

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10.1007/s00769-005-0928-0

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title = "Quality criteria of the isotope dilution method for the determination of polycyclic aromatic hydrocarbons, petroleum-derived hydrocarbons and phenol in leachate of large-scale lysimeter experiments",

abstract = "A comprehensive analytical procedure for polycyclic aromatic hydrocarbons, petroleum-derived hydrocarbons and phenol using the isotope dilution method and employing high-resolution gas chromatography and mass spectrometry was developed and validated for leachates from source-term experiments and the different sampling sites of lysimeters. The use of glassware and other materials is efficiently limited to minimize the risk of contamination. The relative standard deviation elaborated allows precise reliable measurements. Limit of detection and recovery data are useful to judge the quality of each single measurement.",

keywords = "High-resolution gas chromatography-mass spectrometry, Leachate, Lysimeter, Petroleum-derived hydrocarbons, Phenol, Polycyclic aromatic hydrocarbons, Validation",

author = "Schramm, {Karl Werner} and Bernhard Henkelmann and Daniela Peschke and Dieter Martens",

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language = "English",

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Quality criteria of the isotope dilution method for the determination of polycyclic aromatic hydrocarbons, petroleum-derived hydrocarbons and phenol in leachate of large-scale lysimeter experiments. / Schramm, Karl Werner; Henkelmann, Bernhard; Peschke, Daniela et al.
In: Accreditation and Quality Assurance, Vol. 10, No. 5, 05.2005, p. 229-234.

Research output: Contribution to journal › Article › peer-review

TY - JOUR

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AU - Schramm, Karl Werner

AU - Henkelmann, Bernhard

AU - Peschke, Daniela

AU - Martens, Dieter

PY - 2005/5

Y1 - 2005/5

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AB - A comprehensive analytical procedure for polycyclic aromatic hydrocarbons, petroleum-derived hydrocarbons and phenol using the isotope dilution method and employing high-resolution gas chromatography and mass spectrometry was developed and validated for leachates from source-term experiments and the different sampling sites of lysimeters. The use of glassware and other materials is efficiently limited to minimize the risk of contamination. The relative standard deviation elaborated allows precise reliable measurements. Limit of detection and recovery data are useful to judge the quality of each single measurement.

KW - High-resolution gas chromatography-mass spectrometry

KW - Leachate

KW - Lysimeter

KW - Petroleum-derived hydrocarbons

KW - Phenol

KW - Polycyclic aromatic hydrocarbons

KW - Validation

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ER -

Quality criteria of the isotope dilution method for the determination of polycyclic aromatic hydrocarbons, petroleum-derived hydrocarbons and phenol in leachate of large-scale lysimeter experiments

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