PLUSH TACSY: Homonuclear planar TACSY with two-band selective shaped pulses applied to Cα,C′ transfer and Cβ,Caromatic correlations

T. Carlomagno, M. Maurer, M. Sattler, M. G. Schwendinger, S. J. Glaser, C. Griesinger

Research output: Contribution to journalArticlepeer-review

51 Scopus citations

Abstract

A new homonuclear Hartmann-Hahn-type mixing scheme is introduced that effects coherence transfer between resonances in two separated frequency bands. The mixing scheme relies on the irradiation of two-band selective shaped pulses that are expanded in an MLEV-16 supercycle. Similar to heteronuclear Hartmann-Hahn experiments, a planar effective coupling tensor is created. This novel mixing scheme is applied to Cα,C′ transfer and to the transfer between Cβ and aromatic carbon spins.

Original languageEnglish
Pages (from-to)161-170
Number of pages10
JournalJournal of Biomolecular NMR
Volume8
Issue number2
StatePublished - 1996
Externally publishedYes

Keywords

  • Band-selective coherence transfer
  • HEHAHA
  • HOHAHA
  • PLUSH TACSY
  • Sensitivity enhancement

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