Improvement of relayed—NOESY type experiments by implantation of spin‐lock sequences

H. Kessler; G. Gemmecker; B. Haase; S. Steuernagel

doi:10.1002/mrc.1260261018

Improvement of relayed—NOESY type experiments by implantation of spin‐lock sequences

H. Kessler, G. Gemmecker, B. Haase, S. Steuernagel

Johann Wolfgang Goethe University

Research output: Contribution to journal › Article › peer-review

13 Scopus citations

Abstract

Several Relayed—NOESY type pulse sequences are discussed which use spin‐lock periods for one or both of the two transfer steps. The use of such experiments for the sequence analysis of peptides is shown. The requirements for a successful application of special data processing techniques are explained. Even in conformationally rigid peptides where these conditions are no longer fulfilled, the 2D techniques described represent a sensitive and reliable method for the sequential assignment of the spin systems.

Original language	English
Pages (from-to)	919-926
Number of pages	8
Journal	Magnetic Resonance in Chemistry
Volume	26
Issue number	10
DOIs	https://doi.org/10.1002/mrc.1260261018
State	Published - Oct 1988
Externally published	Yes

Keywords

Implantation of spin‐lock sequences
Improved Relayed—NOESEY type pulse sequences
Sequence analysis of peptides

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10.1002/mrc.1260261018

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abstract = "Several Relayed—NOESY type pulse sequences are discussed which use spin‐lock periods for one or both of the two transfer steps. The use of such experiments for the sequence analysis of peptides is shown. The requirements for a successful application of special data processing techniques are explained. Even in conformationally rigid peptides where these conditions are no longer fulfilled, the 2D techniques described represent a sensitive and reliable method for the sequential assignment of the spin systems.",

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year = "1988",

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AU - Gemmecker, G.

AU - Haase, B.

AU - Steuernagel, S.

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AB - Several Relayed—NOESY type pulse sequences are discussed which use spin‐lock periods for one or both of the two transfer steps. The use of such experiments for the sequence analysis of peptides is shown. The requirements for a successful application of special data processing techniques are explained. Even in conformationally rigid peptides where these conditions are no longer fulfilled, the 2D techniques described represent a sensitive and reliable method for the sequential assignment of the spin systems.

KW - Implantation of spin‐lock sequences

KW - Improved Relayed—NOESEY type pulse sequences

KW - Sequence analysis of peptides

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ER -

Improvement of relayed—NOESY type experiments by implantation of spin‐lock sequences

Abstract

Keywords

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