Grazing incidence small angle X-ray scattering on solution cast casein micelle films

Ronald Gebhardt; Charlotte Vendrely; Manfred Burghammer; Christian Riekel; Stephan Volkher Roth; Peter Müller-Buschbaum

doi:10.1557/proc-1147-oo05-05

Grazing incidence small angle X-ray scattering on solution cast casein micelle films

Ronald Gebhardt, Charlotte Vendrely, Manfred Burghammer, Christian Riekel, Stephan Volkher Roth, Peter Müller-Buschbaum

Chair of Functional Materials

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

1 Scopus citations

Abstract

Grazing incidence small angle X-ray scattering with a micrometer sized x-ray beam (so called micro-beam GISAXS, μGISAXS) is used to investigate the microstructure of casein films. Casein micelles treated with rennet enzyme tend to segregate on the surface into a enzyme treated and untreated phase. The biphasic microstructure is monitored by optical microscopy and analyzed by high resolution μGISAXS scans. Furthermore μGISAXS scans provide the possibility to locate highly ordered areas on the casein film surface and to investigate the molecular packing. A simulation via an elastic scattering approach is used to deduce size, dispersion and nearest neighbor distance of the casein micelles embedded in solution casted films. The GISAXS pattern of the highly ordered layer structure of a casein film preparation is shown.

Original language	English
Title of host publication	Grazing-Incidence Small-Angle X-Ray Scattering
Publisher	Materials Research Society
Pages	130-135
Number of pages	6
ISBN (Print)	9781615677733
DOIs	https://doi.org/10.1557/proc-1147-oo05-05
State	Published - 2008
Event	2008 MRS Fall Meeting - Boston, MA, United States Duration: 1 Dec 2008 → 5 Dec 2008

Publication series

Name	Materials Research Society Symposium Proceedings
Volume	1147
ISSN (Print)	0272-9172

Conference

Conference	2008 MRS Fall Meeting
Country/Territory	United States
City	Boston, MA
Period	1/12/08 → 5/12/08

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10.1557/proc-1147-oo05-05

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Gebhardt, R., Vendrely, C., Burghammer, M., Riekel, C., Roth, S. V., & Müller-Buschbaum, P. (2008). Grazing incidence small angle X-ray scattering on solution cast casein micelle films. In Grazing-Incidence Small-Angle X-Ray Scattering (pp. 130-135). (Materials Research Society Symposium Proceedings; Vol. 1147). Materials Research Society. https://doi.org/10.1557/proc-1147-oo05-05

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title = "Grazing incidence small angle X-ray scattering on solution cast casein micelle films",

abstract = "Grazing incidence small angle X-ray scattering with a micrometer sized x-ray beam (so called micro-beam GISAXS, μGISAXS) is used to investigate the microstructure of casein films. Casein micelles treated with rennet enzyme tend to segregate on the surface into a enzyme treated and untreated phase. The biphasic microstructure is monitored by optical microscopy and analyzed by high resolution μGISAXS scans. Furthermore μGISAXS scans provide the possibility to locate highly ordered areas on the casein film surface and to investigate the molecular packing. A simulation via an elastic scattering approach is used to deduce size, dispersion and nearest neighbor distance of the casein micelles embedded in solution casted films. The GISAXS pattern of the highly ordered layer structure of a casein film preparation is shown.",

author = "Ronald Gebhardt and Charlotte Vendrely and Manfred Burghammer and Christian Riekel and Roth, {Stephan Volkher} and Peter M{\"u}ller-Buschbaum",

year = "2008",

doi = "10.1557/proc-1147-oo05-05",

language = "English",

isbn = "9781615677733",

series = "Materials Research Society Symposium Proceedings",

publisher = "Materials Research Society",

pages = "130--135",

booktitle = "Grazing-Incidence Small-Angle X-Ray Scattering",

note = "2008 MRS Fall Meeting ; Conference date: 01-12-2008 Through 05-12-2008",

}

Gebhardt, R, Vendrely, C, Burghammer, M, Riekel, C, Roth, SV & Müller-Buschbaum, P 2008, Grazing incidence small angle X-ray scattering on solution cast casein micelle films. in Grazing-Incidence Small-Angle X-Ray Scattering. Materials Research Society Symposium Proceedings, vol. 1147, Materials Research Society, pp. 130-135, 2008 MRS Fall Meeting, Boston, MA, United States, 1/12/08. https://doi.org/10.1557/proc-1147-oo05-05

Grazing incidence small angle X-ray scattering on solution cast casein micelle films. / Gebhardt, Ronald; Vendrely, Charlotte; Burghammer, Manfred et al.
Grazing-Incidence Small-Angle X-Ray Scattering. Materials Research Society, 2008. p. 130-135 (Materials Research Society Symposium Proceedings; Vol. 1147).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

TY - GEN

T1 - Grazing incidence small angle X-ray scattering on solution cast casein micelle films

AU - Gebhardt, Ronald

AU - Vendrely, Charlotte

AU - Burghammer, Manfred

AU - Riekel, Christian

AU - Roth, Stephan Volkher

AU - Müller-Buschbaum, Peter

PY - 2008

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N2 - Grazing incidence small angle X-ray scattering with a micrometer sized x-ray beam (so called micro-beam GISAXS, μGISAXS) is used to investigate the microstructure of casein films. Casein micelles treated with rennet enzyme tend to segregate on the surface into a enzyme treated and untreated phase. The biphasic microstructure is monitored by optical microscopy and analyzed by high resolution μGISAXS scans. Furthermore μGISAXS scans provide the possibility to locate highly ordered areas on the casein film surface and to investigate the molecular packing. A simulation via an elastic scattering approach is used to deduce size, dispersion and nearest neighbor distance of the casein micelles embedded in solution casted films. The GISAXS pattern of the highly ordered layer structure of a casein film preparation is shown.

AB - Grazing incidence small angle X-ray scattering with a micrometer sized x-ray beam (so called micro-beam GISAXS, μGISAXS) is used to investigate the microstructure of casein films. Casein micelles treated with rennet enzyme tend to segregate on the surface into a enzyme treated and untreated phase. The biphasic microstructure is monitored by optical microscopy and analyzed by high resolution μGISAXS scans. Furthermore μGISAXS scans provide the possibility to locate highly ordered areas on the casein film surface and to investigate the molecular packing. A simulation via an elastic scattering approach is used to deduce size, dispersion and nearest neighbor distance of the casein micelles embedded in solution casted films. The GISAXS pattern of the highly ordered layer structure of a casein film preparation is shown.

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M3 - Conference contribution

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SN - 9781615677733

T3 - Materials Research Society Symposium Proceedings

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BT - Grazing-Incidence Small-Angle X-Ray Scattering

PB - Materials Research Society

T2 - 2008 MRS Fall Meeting

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ER -

Grazing incidence small angle X-ray scattering on solution cast casein micelle films

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