Flow at interfaces: A new device for x-ray surface scattering investigations

J. F. Moulin; S. V. Roth; P. Müller-Buschbaum

doi:10.1063/1.2816220

Flow at interfaces: A new device for x-ray surface scattering investigations

J. F. Moulin
, S. V. Roth
, P. Müller-Buschbaum

Chair of Functional Materials

Research output: Contribution to journal › Article › peer-review

20 Scopus citations

Abstract

A fluidic cell based setup is described which allows for microbeam grazing incidence small angle x-ray scattering characterization of the interface between a solid substrate and a flowing liquid. This cell can potentially be used to study in situ a wide variety of systems ranging from synthetic and natural colloids to biological molecules. The selected channel geometry enables the characterization of the solid-liquid interface during mixing of different solutions. As a proof of concept, measurements on an aqueous gold nanoparticle solution in contact with a glass surface are presented that show that the structure at the interface can be probed during flow.

Original language	English
Article number	015109
Journal	Review of Scientific Instruments
Volume	79
Issue number	1
DOIs	https://doi.org/10.1063/1.2816220
State	Published - 2008

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@article{23031cf901e34dfe9972b57dfad6ee9e,

title = "Flow at interfaces: A new device for x-ray surface scattering investigations",

abstract = "A fluidic cell based setup is described which allows for microbeam grazing incidence small angle x-ray scattering characterization of the interface between a solid substrate and a flowing liquid. This cell can potentially be used to study in situ a wide variety of systems ranging from synthetic and natural colloids to biological molecules. The selected channel geometry enables the characterization of the solid-liquid interface during mixing of different solutions. As a proof of concept, measurements on an aqueous gold nanoparticle solution in contact with a glass surface are presented that show that the structure at the interface can be probed during flow.",

author = "Moulin, \{J. F.\} and Roth, \{S. V.\} and P. M{\"u}ller-Buschbaum",

note = "Funding Information: We thank A. Timmann for the support during the setup of the beamline BW4 and E. Metwalli and W. Wang for their help during the scattering experiments. This work was financially supported by DFG in the priority program for nano- and microfluidics SPP1164 (Grant No. MU1487/2).",

year = "2008",

doi = "10.1063/1.2816220",

language = "English",

volume = "79",

journal = "Review of Scientific Instruments",

issn = "0034-6748",

publisher = "American Institute of Physics",

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T1 - Flow at interfaces

T2 - A new device for x-ray surface scattering investigations

AU - Moulin, J. F.

AU - Roth, S. V.

AU - Müller-Buschbaum, P.

N1 - Funding Information: We thank A. Timmann for the support during the setup of the beamline BW4 and E. Metwalli and W. Wang for their help during the scattering experiments. This work was financially supported by DFG in the priority program for nano- and microfluidics SPP1164 (Grant No. MU1487/2).

PY - 2008

Y1 - 2008

N2 - A fluidic cell based setup is described which allows for microbeam grazing incidence small angle x-ray scattering characterization of the interface between a solid substrate and a flowing liquid. This cell can potentially be used to study in situ a wide variety of systems ranging from synthetic and natural colloids to biological molecules. The selected channel geometry enables the characterization of the solid-liquid interface during mixing of different solutions. As a proof of concept, measurements on an aqueous gold nanoparticle solution in contact with a glass surface are presented that show that the structure at the interface can be probed during flow.

AB - A fluidic cell based setup is described which allows for microbeam grazing incidence small angle x-ray scattering characterization of the interface between a solid substrate and a flowing liquid. This cell can potentially be used to study in situ a wide variety of systems ranging from synthetic and natural colloids to biological molecules. The selected channel geometry enables the characterization of the solid-liquid interface during mixing of different solutions. As a proof of concept, measurements on an aqueous gold nanoparticle solution in contact with a glass surface are presented that show that the structure at the interface can be probed during flow.

UR - https://www.scopus.com/pages/publications/38849134103

U2 - 10.1063/1.2816220

DO - 10.1063/1.2816220

M3 - Article

AN - SCOPUS:38849134103

SN - 0034-6748

VL - 79

JO - Review of Scientific Instruments

JF - Review of Scientific Instruments

IS - 1

M1 - 015109

ER -

Flow at interfaces: A new device for x-ray surface scattering investigations

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