Fast Heteronuclear 3D NMR Spectroscopy

Peter Schmieder; Horst Kessler; Hartmut Oschkinat

doi:10.1002/anie.199005461

Fast Heteronuclear 3D NMR Spectroscopy

Peter Schmieder, Horst Kessler, Hartmut Oschkinat

TUM Emeriti of Excellence

Research output: Contribution to journal › Article › peer-review

15 Scopus citations

Abstract

Carbon atom correlations become interesting in 3D NMR spectroscopy if one selects CH₂ groups with an inverse DEPT sequence in such a way that the spectral breadth in two of the dimensions is limited. 3 D DEPT‐TOCSY has made it possible to obtain, within about ten hours and with a very good signal‐to‐noise ratio, a high‐resolution ¹³C‐resolved 3D NMR spectrum of a cyclic hexapeptide.

Original language	English
Pages (from-to)	546-548
Number of pages	3
Journal	Angewandte Chemie International Edition in English
Volume	29
Issue number	5
DOIs	https://doi.org/10.1002/anie.199005461
State	Published - May 1990

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title = "Fast Heteronuclear 3D NMR Spectroscopy",

abstract = "Carbon atom correlations become interesting in 3D NMR spectroscopy if one selects CH2 groups with an inverse DEPT sequence in such a way that the spectral breadth in two of the dimensions is limited. 3 D DEPT‐TOCSY has made it possible to obtain, within about ten hours and with a very good signal‐to‐noise ratio, a high‐resolution 13C‐resolved 3D NMR spectrum of a cyclic hexapeptide.",

author = "Peter Schmieder and Horst Kessler and Hartmut Oschkinat",

year = "1990",

month = may,

doi = "10.1002/anie.199005461",

language = "English",

volume = "29",

pages = "546--548",

journal = "Angewandte Chemie International Edition in English",

issn = "0570-0833",

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T1 - Fast Heteronuclear 3D NMR Spectroscopy

AU - Schmieder, Peter

AU - Kessler, Horst

AU - Oschkinat, Hartmut

PY - 1990/5

Y1 - 1990/5

N2 - Carbon atom correlations become interesting in 3D NMR spectroscopy if one selects CH2 groups with an inverse DEPT sequence in such a way that the spectral breadth in two of the dimensions is limited. 3 D DEPT‐TOCSY has made it possible to obtain, within about ten hours and with a very good signal‐to‐noise ratio, a high‐resolution 13C‐resolved 3D NMR spectrum of a cyclic hexapeptide.

AB - Carbon atom correlations become interesting in 3D NMR spectroscopy if one selects CH2 groups with an inverse DEPT sequence in such a way that the spectral breadth in two of the dimensions is limited. 3 D DEPT‐TOCSY has made it possible to obtain, within about ten hours and with a very good signal‐to‐noise ratio, a high‐resolution 13C‐resolved 3D NMR spectrum of a cyclic hexapeptide.

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U2 - 10.1002/anie.199005461

DO - 10.1002/anie.199005461

M3 - Article

AN - SCOPUS:33748215689

SN - 0570-0833

VL - 29

SP - 546

EP - 548

JO - Angewandte Chemie International Edition in English

JF - Angewandte Chemie International Edition in English

IS - 5

ER -

Fast Heteronuclear 3D NMR Spectroscopy

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