Dicyclohexylbis(naphthalen-1-ylmethyl)phosphonium chloride chloroform disolvate

Saravanan Gowrisankar, Helfried Neumann, Anke Spannenberg, Matthias Beller

Research output: Contribution to journalArticlepeer-review

1 Scopus citations

Abstract

In the title solvated phosphonium salt, C34H40P+·Cl -·2CHCl3, the two cyclohexyl and two 1-naphthylmethyl groups at the P atom are in a distorted tetrahedral arrangement [105.26 (6)-113.35 (6)°]. Both cyclohexyl rings adopt a chair conformation. The dihedral angle between the naphthyl ring systems is 74.08 (3)°.

Original languageEnglish
Pages (from-to)o3373
JournalActa Crystallographica Section E: Structure Reports Online
Volume68
Issue number12
DOIs
StatePublished - Dec 2012
Externally publishedYes

Keywords

  • R factor = 0.030
  • T = 150 K
  • data-to-parameter ratio = 22.3
  • mean ω(C-C) = 0.002 Å
  • single-crystal X-ray study
  • wR factor = 0.080

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