Deuterated polymer gels for measuring anisotropic NMR parameters with strongly reduced artefacts

Grit Kummerlöwe; Sebastian Knör; Andreas O. Frank; Thomas Paululat; Horst Kessler; Burkhard Luy

doi:10.1039/b812905c

Deuterated polymer gels for measuring anisotropic NMR parameters with strongly reduced artefacts

Grit Kummerlöwe
, Sebastian Knör
, Andreas O. Frank
, Thomas Paululat
, Horst Kessler
, Burkhard Luy

TUM Emeriti of Excellence

Technical University of Munich
University of Siegen

Research output: Contribution to journal › Article › peer-review

32 Scopus citations

Abstract

Perdeuterated poly(styrene) is introduced as an almost artefact-free and arbitrarily scalable alignment medium for measuring residual dipolar couplings and other anisotropic NMR parameters; the spectral quality achievable in this new medium is demonstrated for HSQC spectra leading to the conformational analysis of staurosporine and homonuclear TOCSY-type experiments.

Original language	English
Pages (from-to)	5722-5724
Number of pages	3
Journal	Chemical Communications
Issue number	44
DOIs	https://doi.org/10.1039/b812905c
State	Published - 2008

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title = "Deuterated polymer gels for measuring anisotropic NMR parameters with strongly reduced artefacts",

abstract = "Perdeuterated poly(styrene) is introduced as an almost artefact-free and arbitrarily scalable alignment medium for measuring residual dipolar couplings and other anisotropic NMR parameters; the spectral quality achievable in this new medium is demonstrated for HSQC spectra leading to the conformational analysis of staurosporine and homonuclear TOCSY-type experiments.",

author = "Grit Kummerl{\"o}we and Sebastian Kn{\"o}r and Frank, \{Andreas O.\} and Thomas Paululat and Horst Kessler and Burkhard Luy",

year = "2008",

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journal = "Chemical Communications",

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T1 - Deuterated polymer gels for measuring anisotropic NMR parameters with strongly reduced artefacts

AU - Kummerlöwe, Grit

AU - Knör, Sebastian

AU - Frank, Andreas O.

AU - Paululat, Thomas

AU - Kessler, Horst

AU - Luy, Burkhard

PY - 2008

Y1 - 2008

N2 - Perdeuterated poly(styrene) is introduced as an almost artefact-free and arbitrarily scalable alignment medium for measuring residual dipolar couplings and other anisotropic NMR parameters; the spectral quality achievable in this new medium is demonstrated for HSQC spectra leading to the conformational analysis of staurosporine and homonuclear TOCSY-type experiments.

AB - Perdeuterated poly(styrene) is introduced as an almost artefact-free and arbitrarily scalable alignment medium for measuring residual dipolar couplings and other anisotropic NMR parameters; the spectral quality achievable in this new medium is demonstrated for HSQC spectra leading to the conformational analysis of staurosporine and homonuclear TOCSY-type experiments.

UR - https://www.scopus.com/pages/publications/56349084648

U2 - 10.1039/b812905c

DO - 10.1039/b812905c

M3 - Article

C2 - 19009060

AN - SCOPUS:56349084648

SN - 1359-7345

SP - 5722

EP - 5724

JO - Chemical Communications

JF - Chemical Communications

IS - 44

ER -

Deuterated polymer gels for measuring anisotropic NMR parameters with strongly reduced artefacts

Abstract

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