Deuterated polymer gels for measuring anisotropic NMR parameters with strongly reduced artefacts

Grit Kummerlöwe; Sebastian Knör; Andreas O. Frank; Thomas Paululat; Horst Kessler; Burkhard Luy

doi:10.1039/b812905c

Deuterated polymer gels for measuring anisotropic NMR parameters with strongly reduced artefacts

Grit Kummerlöwe, Sebastian Knör, Andreas O. Frank, Thomas Paululat, Horst Kessler, Burkhard Luy

TUM Emeriti of Excellence

Research output: Contribution to journal › Article › peer-review

31 Scopus citations

Abstract

Perdeuterated poly(styrene) is introduced as an almost artefact-free and arbitrarily scalable alignment medium for measuring residual dipolar couplings and other anisotropic NMR parameters; the spectral quality achievable in this new medium is demonstrated for HSQC spectra leading to the conformational analysis of staurosporine and homonuclear TOCSY-type experiments.

Original language	English
Pages (from-to)	5722-5724
Number of pages	3
Journal	Chemical Communications
Issue number	44
DOIs	https://doi.org/10.1039/b812905c
State	Published - 2008

Access to Document

10.1039/b812905c

Cite this

@article{0a82b573ecf549b3884efabd9e92b790,

title = "Deuterated polymer gels for measuring anisotropic NMR parameters with strongly reduced artefacts",

abstract = "Perdeuterated poly(styrene) is introduced as an almost artefact-free and arbitrarily scalable alignment medium for measuring residual dipolar couplings and other anisotropic NMR parameters; the spectral quality achievable in this new medium is demonstrated for HSQC spectra leading to the conformational analysis of staurosporine and homonuclear TOCSY-type experiments.",

author = "Grit Kummerl{\"o}we and Sebastian Kn{\"o}r and Frank, {Andreas O.} and Thomas Paululat and Horst Kessler and Burkhard Luy",

year = "2008",

doi = "10.1039/b812905c",

language = "English",

pages = "5722--5724",

journal = "Chemical Communications",

issn = "1359-7345",

publisher = "Royal Society of Chemistry",

number = "44",

}

TY - JOUR

T1 - Deuterated polymer gels for measuring anisotropic NMR parameters with strongly reduced artefacts

AU - Kummerlöwe, Grit

AU - Knör, Sebastian

AU - Frank, Andreas O.

AU - Paululat, Thomas

AU - Kessler, Horst

AU - Luy, Burkhard

PY - 2008

Y1 - 2008

N2 - Perdeuterated poly(styrene) is introduced as an almost artefact-free and arbitrarily scalable alignment medium for measuring residual dipolar couplings and other anisotropic NMR parameters; the spectral quality achievable in this new medium is demonstrated for HSQC spectra leading to the conformational analysis of staurosporine and homonuclear TOCSY-type experiments.

AB - Perdeuterated poly(styrene) is introduced as an almost artefact-free and arbitrarily scalable alignment medium for measuring residual dipolar couplings and other anisotropic NMR parameters; the spectral quality achievable in this new medium is demonstrated for HSQC spectra leading to the conformational analysis of staurosporine and homonuclear TOCSY-type experiments.

UR - http://www.scopus.com/inward/record.url?scp=56349084648&partnerID=8YFLogxK

U2 - 10.1039/b812905c

DO - 10.1039/b812905c

M3 - Article

C2 - 19009060

AN - SCOPUS:56349084648

SN - 1359-7345

SP - 5722

EP - 5724

JO - Chemical Communications

JF - Chemical Communications

IS - 44

ER -

Deuterated polymer gels for measuring anisotropic NMR parameters with strongly reduced artefacts

Abstract

Access to Document

Other files and links

Fingerprint

Cite this