Crystal structure of di[potassium(diaza-18-crown-6)]dicaesium nonastannide(4-) diethylenediamine, [K(C12H26N 2O4)]2Cs2[Sn9] · 2C2N2H8, a polyanion∝ 2[KCs2Sn9]- with low-dimensional arrangement of [Sn9] clusters

R. Hauptmann; T. F. Fässler

doi:10.1524/ncrs.2003.218.4.455

Crystal structure of di[potassium(diaza-18-crown-6)]dicaesium nonastannide(4-) diethylenediamine, [K(C₁₂H₂₆N ₂O₄)]₂Cs₂[Sn₉] · 2C₂N₂H₈, a polyanion_∝ ²[KCs₂Sn₉]^- with low-dimensional arrangement of [Sn₉] clusters

R. Hauptmann, T. F. Fässler

Technische Universität Darmstadt

Research output: Contribution to journal › Article › peer-review

11 Scopus citations

Abstract

C₂₈H₆₈CS₂K₂N₈O ₈Sn₉, monoclinic, P12₁/c1 (No. 14), a= 13.897(3) Å, b = 16.091(3)Å, c = 26.432(5) Å, β = 91.03(3)°, V = 5909.7 Å³, Z=4, R_gt(F) = 0.050, wR_ref(F²)= 0.127, T = 153 K.

Original language	English
Pages (from-to)	455-457
Number of pages	3
Journal	Zeitschrift fur Kristallographie - New Crystal Structures
Volume	218
Issue number	4
DOIs	https://doi.org/10.1524/ncrs.2003.218.4.455
State	Published - 2003
Externally published	Yes

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Hauptmann, R., & Fässler, T. F. (2003). Crystal structure of di[potassium(diaza-18-crown-6)]dicaesium nonastannide(4-) diethylenediamine, [K(C₁₂H₂₆N ₂O₄)]₂Cs₂[Sn₉] · 2C₂N₂H₈, a polyanion_∝ ²[KCs₂Sn₉]^- with low-dimensional arrangement of [Sn₉] clusters. Zeitschrift fur Kristallographie - New Crystal Structures, 218(4), 455-457. https://doi.org/10.1524/ncrs.2003.218.4.455

@article{46fd60d24c4e4b6e8bf5a2e608102328,

title = "Crystal structure of di[potassium(diaza-18-crown-6)]dicaesium nonastannide(4-) diethylenediamine, [K(C12H26N 2O4)]2Cs2[Sn9] · 2C2N2H8, a polyanion∝ 2[KCs2Sn9]- with low-dimensional arrangement of [Sn9] clusters",

abstract = "C28H68CS2K2N8O 8Sn9, monoclinic, P121/c1 (No. 14), a= 13.897(3) {\AA}, b = 16.091(3){\AA}, c = 26.432(5) {\AA}, β = 91.03(3)°, V = 5909.7 {\AA}3, Z=4, Rgt(F) = 0.050, wRref(F2)= 0.127, T = 153 K.",

author = "R. Hauptmann and F{\"a}ssler, {T. F.}",

note = "Funding Information: Acknowledgment. This work was supported by the Deutsche Forschungs-gemeinschaft (SPP 1072).",

year = "2003",

doi = "10.1524/ncrs.2003.218.4.455",

language = "English",

volume = "218",

pages = "455--457",

journal = "Zeitschrift fur Kristallographie - New Crystal Structures",

issn = "1433-7266",

publisher = "Walter de Gruyter GmbH",

number = "4",

}

Hauptmann, R & Fässler, TF 2003, 'Crystal structure of di[potassium(diaza-18-crown-6)]dicaesium nonastannide(4-) diethylenediamine, [K(C₁₂H₂₆N ₂O₄)]₂Cs₂[Sn₉] · 2C₂N₂H₈, a polyanion_∝ ²[KCs₂Sn₉]^- with low-dimensional arrangement of [Sn₉] clusters', Zeitschrift fur Kristallographie - New Crystal Structures, vol. 218, no. 4, pp. 455-457. https://doi.org/10.1524/ncrs.2003.218.4.455

Crystal structure of di[potassium(diaza-18-crown-6)]dicaesium nonastannide(4-) diethylenediamine, [K(C₁₂H₂₆N ₂O₄)]₂Cs₂[Sn₉] · 2C₂N₂H₈, a polyanion_∝ ²[KCs₂Sn₉]^- with low-dimensional arrangement of [Sn₉] clusters. / Hauptmann, R.; Fässler, T. F.
In: Zeitschrift fur Kristallographie - New Crystal Structures, Vol. 218, No. 4, 2003, p. 455-457.

Research output: Contribution to journal › Article › peer-review

TY - JOUR

T1 - Crystal structure of di[potassium(diaza-18-crown-6)]dicaesium nonastannide(4-) diethylenediamine, [K(C12H26N 2O4)]2Cs2[Sn9] · 2C2N2H8, a polyanion∝ 2[KCs2Sn9]- with low-dimensional arrangement of [Sn9] clusters

AU - Hauptmann, R.

AU - Fässler, T. F.

N1 - Funding Information: Acknowledgment. This work was supported by the Deutsche Forschungs-gemeinschaft (SPP 1072).

PY - 2003

Y1 - 2003

N2 - C28H68CS2K2N8O 8Sn9, monoclinic, P121/c1 (No. 14), a= 13.897(3) Å, b = 16.091(3)Å, c = 26.432(5) Å, β = 91.03(3)°, V = 5909.7 Å3, Z=4, Rgt(F) = 0.050, wRref(F2)= 0.127, T = 153 K.

AB - C28H68CS2K2N8O 8Sn9, monoclinic, P121/c1 (No. 14), a= 13.897(3) Å, b = 16.091(3)Å, c = 26.432(5) Å, β = 91.03(3)°, V = 5909.7 Å3, Z=4, Rgt(F) = 0.050, wRref(F2)= 0.127, T = 153 K.

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U2 - 10.1524/ncrs.2003.218.4.455

DO - 10.1524/ncrs.2003.218.4.455

M3 - Article

AN - SCOPUS:33748116189

SN - 1433-7266

VL - 218

SP - 455

EP - 457

JO - Zeitschrift fur Kristallographie - New Crystal Structures

JF - Zeitschrift fur Kristallographie - New Crystal Structures

IS - 4