Crystal structure of (4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]- hexacosane-κ8N2,O6) potassium-di-(1,4,7,10,13,16-hexaoxacyclooctadecane-κ6O) potassium potassium nonastannide ethylenediamine sesquisolvate, [K([2.2.2]crypt)][K(18-crown-6)]2[KSn9](en)1.5, C45H96K4N5O18Sn9

Haiyan He; Wilhelm Klein; Thomas F. Fässler

doi:10.1515/ncrs-2014-9039

Crystal structure of (4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]- hexacosane-κ⁸N₂,O₆) potassium-di-(1,4,7,10,13,16-hexaoxacyclooctadecane-κ⁶O) potassium potassium nonastannide ethylenediamine sesquisolvate, [K([2.2.2]crypt)][K(18-crown-6)]₂[KSn₉](en)_1.5, C₄₅H₉₆K₄N₅O₁₈Sn₉

Haiyan He
, Wilhelm Klein
, Thomas F. Fässler

Chair of Inorganic Chemistry with Focus on New Materials

Technical University of Munich

Research output: Contribution to journal › Article › peer-review

2 Scopus citations

Abstract

C₄₅H₉₆K₄N₅O₁₈Sn₉, triclinic, P1 (no. 2), a = 10.1654(3) Å, b = 18.509(1) Å, c = 20.3683(9) Å, α = 83.232(4)°, β = 81.475(3)°, γ = 82.427(3)°, V = 3737.9 Å³, Z = 2, R_gt(F) = 0.0687, wR_ref(F²) = 0.1527, T = 123 K.

Original language	English
Pages (from-to)	407-410
Number of pages	4
Journal	Zeitschrift fur Kristallographie - New Crystal Structures
Volume	229
Issue number	4
DOIs	https://doi.org/10.1515/ncrs-2014-9039
State	Published - 1 Dec 2014

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He, H., Klein, W., & Fässler, T. F. (2014). Crystal structure of (4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]- hexacosane-κ⁸N₂,O₆) potassium-di-(1,4,7,10,13,16-hexaoxacyclooctadecane-κ⁶O) potassium potassium nonastannide ethylenediamine sesquisolvate, [K([2.2.2]crypt)][K(18-crown-6)]₂[KSn₉](en)_1.5, C₄₅H₉₆K₄N₅O₁₈Sn₉. Zeitschrift fur Kristallographie - New Crystal Structures, 229(4), 407-410. https://doi.org/10.1515/ncrs-2014-9039

He, Haiyan ; Klein, Wilhelm ; Fässler, Thomas F. / Crystal structure of (4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]- hexacosane-κ⁸N₂,O₆) potassium-di-(1,4,7,10,13,16-hexaoxacyclooctadecane-κ⁶O) potassium potassium nonastannide ethylenediamine sesquisolvate, [K([2.2.2]crypt)][K(18-crown-6)]₂[KSn₉](en)_1.5, C₄₅H₉₆K₄N₅O₁₈Sn₉. In: Zeitschrift fur Kristallographie - New Crystal Structures. 2014 ; Vol. 229, No. 4. pp. 407-410.

@article{b51e0a8c96f840958ed88521aeeb892d,

title = "Crystal structure of (4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]- hexacosane-κ8N2,O6) potassium-di-(1,4,7,10,13,16-hexaoxacyclooctadecane-κ6O) potassium potassium nonastannide ethylenediamine sesquisolvate, [K([2.2.2]crypt)][K(18-crown-6)]2[KSn9](en)1.5, C45H96K4N5O18Sn9",

abstract = "C45H96K4N5O18Sn9, triclinic, P1 (no. 2), a = 10.1654(3) {\AA}, b = 18.509(1) {\AA}, c = 20.3683(9) {\AA}, α = 83.232(4)°, β = 81.475(3)°, γ = 82.427(3)°, V = 3737.9 {\AA}3, Z = 2, Rgt(F) = 0.0687, wRref(F2) = 0.1527, T = 123 K.",

author = "Haiyan He and Wilhelm Klein and F{\"a}ssler, \{Thomas F.\}",

note = "Publisher Copyright: {\textcopyright} 2014 by Walter de Gruyter Berlin/Boston.",

year = "2014",

month = dec,

day = "1",

doi = "10.1515/ncrs-2014-9039",

language = "English",

volume = "229",

pages = "407--410",

journal = "Zeitschrift fur Kristallographie - New Crystal Structures",

issn = "1433-7266",

publisher = "Walter de Gruyter GmbH",

number = "4",

}

He, H, Klein, W & Fässler, TF 2014, 'Crystal structure of (4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]- hexacosane-κ⁸N₂,O₆) potassium-di-(1,4,7,10,13,16-hexaoxacyclooctadecane-κ⁶O) potassium potassium nonastannide ethylenediamine sesquisolvate, [K([2.2.2]crypt)][K(18-crown-6)]₂[KSn₉](en)_1.5, C₄₅H₉₆K₄N₅O₁₈Sn₉', Zeitschrift fur Kristallographie - New Crystal Structures, vol. 229, no. 4, pp. 407-410. https://doi.org/10.1515/ncrs-2014-9039

Crystal structure of (4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]- hexacosane-κ⁸N₂,O₆) potassium-di-(1,4,7,10,13,16-hexaoxacyclooctadecane-κ⁶O) potassium potassium nonastannide ethylenediamine sesquisolvate, [K([2.2.2]crypt)][K(18-crown-6)]₂[KSn₉](en)_1.5, C₄₅H₉₆K₄N₅O₁₈Sn₉. / He, Haiyan; Klein, Wilhelm; Fässler, Thomas F.
In: Zeitschrift fur Kristallographie - New Crystal Structures, Vol. 229, No. 4, 01.12.2014, p. 407-410.

Research output: Contribution to journal › Article › peer-review

TY - JOUR

T1 - Crystal structure of (4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]- hexacosane-κ8N2,O6) potassium-di-(1,4,7,10,13,16-hexaoxacyclooctadecane-κ6O) potassium potassium nonastannide ethylenediamine sesquisolvate, [K([2.2.2]crypt)][K(18-crown-6)]2[KSn9](en)1.5, C45H96K4N5O18Sn9

AU - He, Haiyan

AU - Klein, Wilhelm

AU - Fässler, Thomas F.

PY - 2014/12/1

Y1 - 2014/12/1

N2 - C45H96K4N5O18Sn9, triclinic, P1 (no. 2), a = 10.1654(3) Å, b = 18.509(1) Å, c = 20.3683(9) Å, α = 83.232(4)°, β = 81.475(3)°, γ = 82.427(3)°, V = 3737.9 Å3, Z = 2, Rgt(F) = 0.0687, wRref(F2) = 0.1527, T = 123 K.

AB - C45H96K4N5O18Sn9, triclinic, P1 (no. 2), a = 10.1654(3) Å, b = 18.509(1) Å, c = 20.3683(9) Å, α = 83.232(4)°, β = 81.475(3)°, γ = 82.427(3)°, V = 3737.9 Å3, Z = 2, Rgt(F) = 0.0687, wRref(F2) = 0.1527, T = 123 K.

UR - https://www.scopus.com/pages/publications/84919461082

U2 - 10.1515/ncrs-2014-9039

DO - 10.1515/ncrs-2014-9039

M3 - Article

AN - SCOPUS:84919461082

SN - 1433-7266

VL - 229

SP - 407

EP - 410

JO - Zeitschrift fur Kristallographie - New Crystal Structures

JF - Zeitschrift fur Kristallographie - New Crystal Structures

IS - 4

ER -

He H, Klein W, Fässler TF. Crystal structure of (4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]- hexacosane-κ⁸N₂,O₆) potassium-di-(1,4,7,10,13,16-hexaoxacyclooctadecane-κ⁶O) potassium potassium nonastannide ethylenediamine sesquisolvate, [K([2.2.2]crypt)][K(18-crown-6)]₂[KSn₉](en)_1.5, C₄₅H₉₆K₄N₅O₁₈Sn₉. Zeitschrift fur Kristallographie - New Crystal Structures. 2014 Dec 1;229(4):407-410. doi: 10.1515/ncrs-2014-9039

Crystal structure of (4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]- hexacosane-κ8N2,O6) potassium-di-(1,4,7,10,13,16-hexaoxacyclooctadecane-κ6O) potassium potassium nonastannide ethylenediamine sesquisolvate, [K([2.2.2]crypt)][K(18-crown-6)]2[KSn9](en)1.5, C45H96K4N5O18Sn9

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