Crystal structure of (1,4,7,10,13,16-hexaoxacyclooctadecane-κ6O6) 1,2,3,4,5-pentamethyl-cyclopenta-2,4-dien-1-yl(potassium, rubidium) - Ammonia (1/2), [K0.3Rb0.7(18-crown-6)]Cp∗· 2 NH3, C22H45K0.3N2O6Rb0.7

Thomas Henneberger; Wilhelm Klein; Thomas F. Fässler

doi:10.1515/ncrs-2019-0368

Crystal structure of (1,4,7,10,13,16-hexaoxacyclooctadecane-κ⁶O₆) 1,2,3,4,5-pentamethyl-cyclopenta-2,4-dien-1-yl(potassium, rubidium) - Ammonia (1/2), [K_0.3Rb_0.7(18-crown-6)]Cp∗· 2 NH₃, C₂₂H₄₅K_0.3N₂O₆Rb_0.7

Thomas Henneberger, Wilhelm Klein, Thomas F. Fässler

Chair of Inorganic Chemistry with Focus on New Materials

Technical University of Munich

Research output: Contribution to journal › Article › peer-review

2 Scopus citations

Abstract

C₂₂H₄₅K_0.26N₂O₆Rb_0.74, orthorhombic, Pbca (no. 61), a = 10.1587(8) Å, b = 16.2842(15) Å, c = 32.862(3) Å, V = 5436.2(8) Å³, Z = 8, R_gt(F) = 0.0386, wR_ref(F²) = 0.0616, T = 120(2) K.

Original language	English
Journal	Zeitschrift fur Kristallographie - New Crystal Structures
DOIs	https://doi.org/10.1515/ncrs-2019-0368
State	Accepted/In press - 2019

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Henneberger, T., Klein, W., & Fässler, T. F. (Accepted/In press). Crystal structure of (1,4,7,10,13,16-hexaoxacyclooctadecane-κ⁶O₆) 1,2,3,4,5-pentamethyl-cyclopenta-2,4-dien-1-yl(potassium, rubidium) - Ammonia (1/2), [K_0.3Rb_0.7(18-crown-6)]Cp∗· 2 NH₃, C₂₂H₄₅K_0.3N₂O₆Rb_0.7 Zeitschrift fur Kristallographie - New Crystal Structures. https://doi.org/10.1515/ncrs-2019-0368

@article{0f0234ca34ac499fb401f732e839accd,

title = "Crystal structure of (1,4,7,10,13,16-hexaoxacyclooctadecane-κ6O6) 1,2,3,4,5-pentamethyl-cyclopenta-2,4-dien-1-yl(potassium, rubidium) - Ammonia (1/2), [K0.3Rb0.7(18-crown-6)]Cp∗· 2 NH3, C22H45K0.3N2O6Rb0.7 ",

abstract = "C22H45K0.26N2O6Rb0.74, orthorhombic, Pbca (no. 61), a = 10.1587(8) {\AA}, b = 16.2842(15) {\AA}, c = 32.862(3) {\AA}, V = 5436.2(8) {\AA}3, Z = 8, Rgt(F) = 0.0386, wRref(F2) = 0.0616, T = 120(2) K.",

author = "Thomas Henneberger and Wilhelm Klein and F{\"a}ssler, {Thomas F.}",

note = "Funding Information: This work was supported by the Deutsche Forschungsgemeinschaft (DFG) and the Technische Universit{\"a}t M{\"u}nchen within the funding programme Open Access Publishing. Publisher Copyright: {\textcopyright}2019 Thomas Henneberger et al., published by De Gruyter, Berlin/Boston.",

year = "2019",

doi = "10.1515/ncrs-2019-0368",

language = "English",

journal = "Zeitschrift fur Kristallographie - New Crystal Structures",

issn = "1433-7266",

publisher = "Walter de Gruyter GmbH",

}

Henneberger, T, Klein, W & Fässler, TF 2019, 'Crystal structure of (1,4,7,10,13,16-hexaoxacyclooctadecane-κ⁶O₆) 1,2,3,4,5-pentamethyl-cyclopenta-2,4-dien-1-yl(potassium, rubidium) - Ammonia (1/2), [K_0.3Rb_0.7(18-crown-6)]Cp∗· 2 NH₃, C₂₂H₄₅K_0.3N₂O₆Rb_0.7 ', Zeitschrift fur Kristallographie - New Crystal Structures. https://doi.org/10.1515/ncrs-2019-0368

Crystal structure of (1,4,7,10,13,16-hexaoxacyclooctadecane-κ⁶O₆) 1,2,3,4,5-pentamethyl-cyclopenta-2,4-dien-1-yl(potassium, rubidium) - Ammonia (1/2), [K_0.3Rb_0.7(18-crown-6)]Cp∗· 2 NH₃, C₂₂H₄₅K_0.3N₂O₆Rb_0.7 . / Henneberger, Thomas; Klein, Wilhelm; Fässler, Thomas F.
In: Zeitschrift fur Kristallographie - New Crystal Structures, 2019.

Research output: Contribution to journal › Article › peer-review

TY - JOUR

T1 - Crystal structure of (1,4,7,10,13,16-hexaoxacyclooctadecane-κ6O6) 1,2,3,4,5-pentamethyl-cyclopenta-2,4-dien-1-yl(potassium, rubidium) - Ammonia (1/2), [K0.3Rb0.7(18-crown-6)]Cp∗· 2 NH3, C22H45K0.3N2O6Rb0.7

AU - Henneberger, Thomas

AU - Klein, Wilhelm

AU - Fässler, Thomas F.

N1 - Funding Information: This work was supported by the Deutsche Forschungsgemeinschaft (DFG) and the Technische Universität München within the funding programme Open Access Publishing. Publisher Copyright: ©2019 Thomas Henneberger et al., published by De Gruyter, Berlin/Boston.

PY - 2019

Y1 - 2019

N2 - C22H45K0.26N2O6Rb0.74, orthorhombic, Pbca (no. 61), a = 10.1587(8) Å, b = 16.2842(15) Å, c = 32.862(3) Å, V = 5436.2(8) Å3, Z = 8, Rgt(F) = 0.0386, wRref(F2) = 0.0616, T = 120(2) K.

AB - C22H45K0.26N2O6Rb0.74, orthorhombic, Pbca (no. 61), a = 10.1587(8) Å, b = 16.2842(15) Å, c = 32.862(3) Å, V = 5436.2(8) Å3, Z = 8, Rgt(F) = 0.0386, wRref(F2) = 0.0616, T = 120(2) K.

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U2 - 10.1515/ncrs-2019-0368

DO - 10.1515/ncrs-2019-0368

M3 - Article

AN - SCOPUS:85074301643

SN - 1433-7266

JO - Zeitschrift fur Kristallographie - New Crystal Structures

JF - Zeitschrift fur Kristallographie - New Crystal Structures