Crystal structure of (1,4,7,10,13,16-hexaoxacyclooctadecane-κ 6O6)potassium(2-methylphenylamino)ethyl-2-methylphenylamide ammoniate (1/3.5), [K(18-crown-6)](o-CH3C6H4)NH(CH2)2N(o-CH3C6H4) 3.5 NH3, C28H53.5KN5.5O6

Christoph Wallach; Wilhelm Klein; Thomas F. Fässler

doi:10.1515/ncrs-2022-0275

Crystal structure of (1,4,7,10,13,16-hexaoxacyclooctadecane-κ ⁶O₆)potassium(2-methylphenylamino)ethyl-2-methylphenylamide ammoniate (1/3.5), [K(18-crown-6)](o-CH₃C₆H₄)NH(CH₂)₂N(o-CH₃C₆H₄) 3.5 NH₃, C₂₈H_53.5KN_5.5O₆

Christoph Wallach, Wilhelm Klein, Thomas F. Fässler

Chair of Inorganic Chemistry with Focus on New Materials

Technical University of Munich

Research output: Contribution to journal › Article › peer-review

Abstract

C28H53.5KN5.5O6, monoclinic, Pc (no. 7), a = 18.7986(12) Å, b = 8.3431(6) Å, c = 22.4638(16) Å, β = 100.554(5)°, V = 3463.6(4) Å3, Z = 4, Rgt (F) = 0.0712, wRref (F 2) = 0.2226, T = 150 K.

Original language	English
Pages (from-to)	897-901
Number of pages	5
Journal	Zeitschrift fur Kristallographie - New Crystal Structures
Volume	237
Issue number	5
DOIs	https://doi.org/10.1515/ncrs-2022-0275
State	Published - 1 Oct 2022

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Wallach, C., Klein, W., & Fässler, T. F. (2022). Crystal structure of (1,4,7,10,13,16-hexaoxacyclooctadecane-κ ⁶O₆)potassium(2-methylphenylamino)ethyl-2-methylphenylamide ammoniate (1/3.5), [K(18-crown-6)](o-CH₃C₆H₄)NH(CH₂)₂N(o-CH₃C₆H₄) 3.5 NH₃, C₂₈H_53.5KN_5.5O₆. Zeitschrift fur Kristallographie - New Crystal Structures, 237(5), 897-901. https://doi.org/10.1515/ncrs-2022-0275

Wallach, Christoph ; Klein, Wilhelm ; Fässler, Thomas F. / Crystal structure of (1,4,7,10,13,16-hexaoxacyclooctadecane-κ ⁶O₆)potassium(2-methylphenylamino)ethyl-2-methylphenylamide ammoniate (1/3.5), [K(18-crown-6)](o-CH₃C₆H₄)NH(CH₂)₂N(o-CH₃C₆H₄) 3.5 NH₃, C₂₈H_53.5KN_5.5O₆. In: Zeitschrift fur Kristallographie - New Crystal Structures. 2022 ; Vol. 237, No. 5. pp. 897-901.

@article{a7c33141b9d74ff8b3f28f664466554b,

title = "Crystal structure of (1,4,7,10,13,16-hexaoxacyclooctadecane-κ 6O6)potassium(2-methylphenylamino)ethyl-2-methylphenylamide ammoniate (1/3.5), [K(18-crown-6)](o-CH3C6H4)NH(CH2)2N(o-CH3C6H4) 3.5 NH3, C28H53.5KN5.5O6",

abstract = "C28H53.5KN5.5O6, monoclinic, Pc (no. 7), a = 18.7986(12) {\AA}, b = 8.3431(6) {\AA}, c = 22.4638(16) {\AA}, β = 100.554(5)°, V = 3463.6(4) {\AA}3, Z = 4, Rgt (F) = 0.0712, wRref (F 2) = 0.2226, T = 150 K.",

author = "Christoph Wallach and Wilhelm Klein and F{\"a}ssler, {Thomas F.}",

note = "Publisher Copyright: {\textcopyright} 2022 the author(s), published by De Gruyter, Berlin/Boston.",

year = "2022",

month = oct,

day = "1",

doi = "10.1515/ncrs-2022-0275",

language = "English",

volume = "237",

pages = "897--901",

journal = "Zeitschrift fur Kristallographie - New Crystal Structures",

issn = "1433-7266",

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Wallach, C, Klein, W & Fässler, TF 2022, 'Crystal structure of (1,4,7,10,13,16-hexaoxacyclooctadecane-κ ⁶O₆)potassium(2-methylphenylamino)ethyl-2-methylphenylamide ammoniate (1/3.5), [K(18-crown-6)](o-CH₃C₆H₄)NH(CH₂)₂N(o-CH₃C₆H₄) 3.5 NH₃, C₂₈H_53.5KN_5.5O₆', Zeitschrift fur Kristallographie - New Crystal Structures, vol. 237, no. 5, pp. 897-901. https://doi.org/10.1515/ncrs-2022-0275

Crystal structure of (1,4,7,10,13,16-hexaoxacyclooctadecane-κ ⁶O₆)potassium(2-methylphenylamino)ethyl-2-methylphenylamide ammoniate (1/3.5), [K(18-crown-6)](o-CH₃C₆H₄)NH(CH₂)₂N(o-CH₃C₆H₄) 3.5 NH₃, C₂₈H_53.5KN_5.5O₆. / Wallach, Christoph; Klein, Wilhelm; Fässler, Thomas F.
In: Zeitschrift fur Kristallographie - New Crystal Structures, Vol. 237, No. 5, 01.10.2022, p. 897-901.

Research output: Contribution to journal › Article › peer-review

TY - JOUR

T1 - Crystal structure of (1,4,7,10,13,16-hexaoxacyclooctadecane-κ 6O6)potassium(2-methylphenylamino)ethyl-2-methylphenylamide ammoniate (1/3.5), [K(18-crown-6)](o-CH3C6H4)NH(CH2)2N(o-CH3C6H4) 3.5 NH3, C28H53.5KN5.5O6

AU - Wallach, Christoph

AU - Klein, Wilhelm

AU - Fässler, Thomas F.

PY - 2022/10/1

Y1 - 2022/10/1

N2 - C28H53.5KN5.5O6, monoclinic, Pc (no. 7), a = 18.7986(12) Å, b = 8.3431(6) Å, c = 22.4638(16) Å, β = 100.554(5)°, V = 3463.6(4) Å3, Z = 4, Rgt (F) = 0.0712, wRref (F 2) = 0.2226, T = 150 K.

AB - C28H53.5KN5.5O6, monoclinic, Pc (no. 7), a = 18.7986(12) Å, b = 8.3431(6) Å, c = 22.4638(16) Å, β = 100.554(5)°, V = 3463.6(4) Å3, Z = 4, Rgt (F) = 0.0712, wRref (F 2) = 0.2226, T = 150 K.

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U2 - 10.1515/ncrs-2022-0275

DO - 10.1515/ncrs-2022-0275

M3 - Article

AN - SCOPUS:85135781970

SN - 1433-7266

VL - 237

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EP - 901

JO - Zeitschrift fur Kristallographie - New Crystal Structures

JF - Zeitschrift fur Kristallographie - New Crystal Structures

IS - 5