An easy and scalable method for the partial alignment of organic molecules for measuring residual dipolar couplings

Burkhard Luy; Kyryl Kobzar; Horst Kessler

doi:10.1002/anie.200352860

An easy and scalable method for the partial alignment of organic molecules for measuring residual dipolar couplings

Burkhard Luy, Kyryl Kobzar, Horst Kessler

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Technical University of Munich

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103 Scopus citations

Abstract

Stretched polystyrene gel (see picture) induces partial alignment of small molecules in an organic solvent for the measurement of residual dipolar couplings in high-resolution NMR spectroscopy. The degree of orientation can be varied over a wide range by the amount of cross-linking of the polymer. An important NMR parameter can thus be measured routinely.

Original language	English
Pages (from-to)	1092-1094
Number of pages	3
Journal	Angewandte Chemie International Edition in English
Volume	43
Issue number	9
DOIs	https://doi.org/10.1002/anie.200352860
State	Published - 20 Feb 2004

Keywords

Gels
NMR spectroscopy
Partial alignment
Polystyrene
Residual dipolar coupling

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10.1002/anie.200352860

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An easy and scalable method for the partial alignment of organic molecules for measuring residual dipolar couplings

Abstract

Keywords

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