A novel laser-liquid-solid interaction process for hydroxyapatite formation on porous silicon

Liliana Pramatarova; Emilia Pecheva; D. Dimova-Malinovska; Radina Presker; Martin Stutzmann; U. Schwarz; R. Kniep

doi:10.1117/12.618423

A novel laser-liquid-solid interaction process for hydroxyapatite formation on porous silicon

Liliana Pramatarova, Emilia Pecheva, D. Dimova-Malinovska, Radina Presker, Martin Stutzmann, U. Schwarz, R. Kniep

TUM Emeriti of Excellence

Research output: Contribution to journal › Conference article › peer-review

6 Scopus citations

Abstract

The mechanism of hydroxyapatite (HA, Ca₁₀(PO₄)6(OH) ₂) growth on the surface of porous silicon (PS) was examined. PS layers were prepared by electrochemical or chemical etching of n-type Si with (111) orientation, and p-type Si with (100) orientation. HA growth was induced by two methods: a simple soaking process in a simulated body fluid (SBF) and a novel Laser-Liquid-Solid Interaction (LLSI) process which allowed interaction between a scanning laser beam and the PS substrate immersed in the SBF. The grown layers were investigated by light microscopy, electron microprobe analysis, Raman spectroscopy and X-ray diffraction. Differently doped Si substrates with different crystallographic orientation and electrical resistivity were used and their effect on the HA growth, as well as the effect of the laser energy were examined.

Original language	English
Article number	18
Pages (from-to)	110-114
Number of pages	5
Journal	Proceedings of SPIE - The International Society for Optical Engineering
Volume	5830
DOIs	https://doi.org/10.1117/12.618423
State	Published - 2005
Event	13th International School on Quantum Electronics: Laser Physics and Applications - Bourgas, Bulgaria Duration: 20 Sep 2004 → 24 Sep 2004

Keywords

Hydroxyapatite
Laser-liquid-solid interaction
Porous silicon

Access to Document

10.1117/12.618423

Cite this

@article{871b154170f34e3cbfc742947b586620,

title = "A novel laser-liquid-solid interaction process for hydroxyapatite formation on porous silicon",

abstract = "The mechanism of hydroxyapatite (HA, Ca10(PO4)6(OH) 2) growth on the surface of porous silicon (PS) was examined. PS layers were prepared by electrochemical or chemical etching of n-type Si with (111) orientation, and p-type Si with (100) orientation. HA growth was induced by two methods: a simple soaking process in a simulated body fluid (SBF) and a novel Laser-Liquid-Solid Interaction (LLSI) process which allowed interaction between a scanning laser beam and the PS substrate immersed in the SBF. The grown layers were investigated by light microscopy, electron microprobe analysis, Raman spectroscopy and X-ray diffraction. Differently doped Si substrates with different crystallographic orientation and electrical resistivity were used and their effect on the HA growth, as well as the effect of the laser energy were examined.",

keywords = "Hydroxyapatite, Laser-liquid-solid interaction, Porous silicon",

author = "Liliana Pramatarova and Emilia Pecheva and D. Dimova-Malinovska and Radina Presker and Martin Stutzmann and U. Schwarz and R. Kniep",

year = "2005",

doi = "10.1117/12.618423",

language = "English",

volume = "5830",

pages = "110--114",

journal = "Proceedings of SPIE - The International Society for Optical Engineering",

issn = "0277-786X",

publisher = "SPIE",

note = "13th International School on Quantum Electronics: Laser Physics and Applications ; Conference date: 20-09-2004 Through 24-09-2004",

}

TY - JOUR

T1 - A novel laser-liquid-solid interaction process for hydroxyapatite formation on porous silicon

AU - Pramatarova, Liliana

AU - Pecheva, Emilia

AU - Dimova-Malinovska, D.

AU - Presker, Radina

AU - Stutzmann, Martin

AU - Schwarz, U.

AU - Kniep, R.

PY - 2005

Y1 - 2005

N2 - The mechanism of hydroxyapatite (HA, Ca10(PO4)6(OH) 2) growth on the surface of porous silicon (PS) was examined. PS layers were prepared by electrochemical or chemical etching of n-type Si with (111) orientation, and p-type Si with (100) orientation. HA growth was induced by two methods: a simple soaking process in a simulated body fluid (SBF) and a novel Laser-Liquid-Solid Interaction (LLSI) process which allowed interaction between a scanning laser beam and the PS substrate immersed in the SBF. The grown layers were investigated by light microscopy, electron microprobe analysis, Raman spectroscopy and X-ray diffraction. Differently doped Si substrates with different crystallographic orientation and electrical resistivity were used and their effect on the HA growth, as well as the effect of the laser energy were examined.

AB - The mechanism of hydroxyapatite (HA, Ca10(PO4)6(OH) 2) growth on the surface of porous silicon (PS) was examined. PS layers were prepared by electrochemical or chemical etching of n-type Si with (111) orientation, and p-type Si with (100) orientation. HA growth was induced by two methods: a simple soaking process in a simulated body fluid (SBF) and a novel Laser-Liquid-Solid Interaction (LLSI) process which allowed interaction between a scanning laser beam and the PS substrate immersed in the SBF. The grown layers were investigated by light microscopy, electron microprobe analysis, Raman spectroscopy and X-ray diffraction. Differently doped Si substrates with different crystallographic orientation and electrical resistivity were used and their effect on the HA growth, as well as the effect of the laser energy were examined.

KW - Hydroxyapatite

KW - Laser-liquid-solid interaction

KW - Porous silicon

UR - http://www.scopus.com/inward/record.url?scp=27744508675&partnerID=8YFLogxK

U2 - 10.1117/12.618423

DO - 10.1117/12.618423

M3 - Conference article

AN - SCOPUS:27744508675

SN - 0277-786X

VL - 5830

SP - 110

EP - 114

JO - Proceedings of SPIE - The International Society for Optical Engineering

JF - Proceedings of SPIE - The International Society for Optical Engineering

M1 - 18

T2 - 13th International School on Quantum Electronics: Laser Physics and Applications

Y2 - 20 September 2004 through 24 September 2004

ER -

A novel laser-liquid-solid interaction process for hydroxyapatite formation on porous silicon

Abstract

Keywords

Access to Document

Other files and links

Fingerprint

Cite this