Influence of fluid dynamics on the electrochemical deposition of tantalum

S. Martens; A. Ispas; L. Asen; L. Seidl; U. Stimming; O. Schneider; A. Bund

doi:10.1149/07515.0287ecst

Influence of fluid dynamics on the electrochemical deposition of tantalum

S. Martens, A. Ispas, L. Asen, L. Seidl, U. Stimming, O. Schneider, A. Bund

Publikation: Beitrag in Buch/Bericht/Konferenzband › Konferenzbeitrag › Begutachtung

3 Zitate (Scopus)

Abstract

In the electrochemical deposition of Tantalum from ionic liquids at moderate temperatures, the preparation of purely metallic coatings with thicknesses in the micrometer range and the accurate control of the crystallographic parameters remain challenging. In this work, preliminary experiments on the influence of fluid dynamics during the electrodeposition of tantalum in the ionic liquid 1-butyl-1-methylpyrrolidinium bis(trifluoromethylsulfonyl) imide using ultrasound as an additional source of energy were carried out. This included a study on the influence of the ultrasound amplitude on the deposition rate of tantalum by using cyclic voltammetry and the in-situ electrochemical quartz crystal microbalance technique.

Originalsprache	Englisch
Titel	Molten Salts and Ionic Liquids 20
Redakteure/-innen	L. M. Haverhals, R. A. Mantz, P. C. Trulove, M. Ueda, M. Carter, E. J. Biddinger, A. H. Suroviec, M. Reichert, F. Endres, A. Bund, A. Ispas, D. M. Fox, H. C. De Long
Herausgeber (Verlag)	Electrochemical Society Inc.
Seiten	287-295
Seitenumfang	9
Auflage	15
ISBN (elektronisch)	9781607687320, 9781607687672, 9781607687689, 9781607687696, 9781607687702, 9781607687719, 9781607687726, 9781607687733, 9781607687740, 9781607687757, 9781607687771, 9781607687788, 9781607687795, 9781607687801, 9781607687818, 9781607687825, 9781607687832, 9781607687849, 9781607687856, 9781607687863, 9781607687887, 9781607687894, 9781607687900, 9781607687917, 9781607687924, 9781607687931, 9781607687948, 9781607687955, 9781607687962, 9781607687979, 9781607687986, 9781607687993, 9781607688006, 9781607688013, 9781607688020, 9781607688037
DOIs	https://doi.org/10.1149/07515.0287ecst
Publikationsstatus	Veröffentlicht - 2016
Extern publiziert	Ja
Veranstaltung	Symposium on Molten Salts and Ionic Liquids 20 - PRiME 2016/230th ECS Meeting - Honolulu, USA/Vereinigte Staaten Dauer: 2 Okt. 2016 → 7 Okt. 2016

Publikationsreihe

Name	ECS Transactions
Nummer	15
Band	75
ISSN (Print)	1938-6737
ISSN (elektronisch)	1938-5862

Konferenz

Konferenz	Symposium on Molten Salts and Ionic Liquids 20 - PRiME 2016/230th ECS Meeting
Land/Gebiet	USA/Vereinigte Staaten
Ort	Honolulu
Zeitraum	2/10/16 → 7/10/16

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10.1149/07515.0287ecst

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Martens, S., Ispas, A., Asen, L., Seidl, L., Stimming, U., Schneider, O., & Bund, A. (2016). Influence of fluid dynamics on the electrochemical deposition of tantalum. in L. M. Haverhals, R. A. Mantz, P. C. Trulove, M. Ueda, M. Carter, E. J. Biddinger, A. H. Suroviec, M. Reichert, F. Endres, A. Bund, A. Ispas, D. M. Fox, & H. C. De Long (Hrsg.), Molten Salts and Ionic Liquids 20 (15 Aufl., S. 287-295). (ECS Transactions; Band 75, Nr. 15). Electrochemical Society Inc.. https://doi.org/10.1149/07515.0287ecst

Martens, S. ; Ispas, A. ; Asen, L. et al. / Influence of fluid dynamics on the electrochemical deposition of tantalum. Molten Salts and Ionic Liquids 20. Hrsg. / L. M. Haverhals ; R. A. Mantz ; P. C. Trulove ; M. Ueda ; M. Carter ; E. J. Biddinger ; A. H. Suroviec ; M. Reichert ; F. Endres ; A. Bund ; A. Ispas ; D. M. Fox ; H. C. De Long. 15. Aufl. Electrochemical Society Inc., 2016. S. 287-295 (ECS Transactions; 15).

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title = "Influence of fluid dynamics on the electrochemical deposition of tantalum",

abstract = "In the electrochemical deposition of Tantalum from ionic liquids at moderate temperatures, the preparation of purely metallic coatings with thicknesses in the micrometer range and the accurate control of the crystallographic parameters remain challenging. In this work, preliminary experiments on the influence of fluid dynamics during the electrodeposition of tantalum in the ionic liquid 1-butyl-1-methylpyrrolidinium bis(trifluoromethylsulfonyl) imide using ultrasound as an additional source of energy were carried out. This included a study on the influence of the ultrasound amplitude on the deposition rate of tantalum by using cyclic voltammetry and the in-situ electrochemical quartz crystal microbalance technique.",

author = "S. Martens and A. Ispas and L. Asen and L. Seidl and U. Stimming and O. Schneider and A. Bund",

year = "2016",

doi = "10.1149/07515.0287ecst",

language = "English",

series = "ECS Transactions",

publisher = "Electrochemical Society Inc.",

number = "15",

pages = "287--295",

editor = "Haverhals, {L. M.} and Mantz, {R. A.} and Trulove, {P. C.} and M. Ueda and M. Carter and Biddinger, {E. J.} and Suroviec, {A. H.} and M. Reichert and F. Endres and A. Bund and A. Ispas and Fox, {D. M.} and {De Long}, {H. C.}",

booktitle = "Molten Salts and Ionic Liquids 20",

edition = "15",

note = "Symposium on Molten Salts and Ionic Liquids 20 - PRiME 2016/230th ECS Meeting ; Conference date: 02-10-2016 Through 07-10-2016",

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Martens, S, Ispas, A, Asen, L, Seidl, L, Stimming, U, Schneider, O & Bund, A 2016, Influence of fluid dynamics on the electrochemical deposition of tantalum. in LM Haverhals, RA Mantz, PC Trulove, M Ueda, M Carter, EJ Biddinger, AH Suroviec, M Reichert, F Endres, A Bund, A Ispas, DM Fox & HC De Long (Hrsg.), Molten Salts and Ionic Liquids 20. 15 Aufl., ECS Transactions, Nr. 15, Bd. 75, Electrochemical Society Inc., S. 287-295, Symposium on Molten Salts and Ionic Liquids 20 - PRiME 2016/230th ECS Meeting, Honolulu, USA/Vereinigte Staaten, 2/10/16. https://doi.org/10.1149/07515.0287ecst

Influence of fluid dynamics on the electrochemical deposition of tantalum. / Martens, S.; Ispas, A.; Asen, L. et al.
Molten Salts and Ionic Liquids 20. Hrsg. / L. M. Haverhals; R. A. Mantz; P. C. Trulove; M. Ueda; M. Carter; E. J. Biddinger; A. H. Suroviec; M. Reichert; F. Endres; A. Bund; A. Ispas; D. M. Fox; H. C. De Long. 15. Aufl. Electrochemical Society Inc., 2016. S. 287-295 (ECS Transactions; Band 75, Nr. 15).

Publikation: Beitrag in Buch/Bericht/Konferenzband › Konferenzbeitrag › Begutachtung

TY - GEN

T1 - Influence of fluid dynamics on the electrochemical deposition of tantalum

AU - Martens, S.

AU - Ispas, A.

AU - Asen, L.

AU - Seidl, L.

AU - Stimming, U.

AU - Schneider, O.

AU - Bund, A.

PY - 2016

Y1 - 2016

N2 - In the electrochemical deposition of Tantalum from ionic liquids at moderate temperatures, the preparation of purely metallic coatings with thicknesses in the micrometer range and the accurate control of the crystallographic parameters remain challenging. In this work, preliminary experiments on the influence of fluid dynamics during the electrodeposition of tantalum in the ionic liquid 1-butyl-1-methylpyrrolidinium bis(trifluoromethylsulfonyl) imide using ultrasound as an additional source of energy were carried out. This included a study on the influence of the ultrasound amplitude on the deposition rate of tantalum by using cyclic voltammetry and the in-situ electrochemical quartz crystal microbalance technique.

AB - In the electrochemical deposition of Tantalum from ionic liquids at moderate temperatures, the preparation of purely metallic coatings with thicknesses in the micrometer range and the accurate control of the crystallographic parameters remain challenging. In this work, preliminary experiments on the influence of fluid dynamics during the electrodeposition of tantalum in the ionic liquid 1-butyl-1-methylpyrrolidinium bis(trifluoromethylsulfonyl) imide using ultrasound as an additional source of energy were carried out. This included a study on the influence of the ultrasound amplitude on the deposition rate of tantalum by using cyclic voltammetry and the in-situ electrochemical quartz crystal microbalance technique.

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U2 - 10.1149/07515.0287ecst

DO - 10.1149/07515.0287ecst

M3 - Conference contribution

AN - SCOPUS:84991327751

T3 - ECS Transactions

SP - 287

EP - 295

BT - Molten Salts and Ionic Liquids 20

A2 - Haverhals, L. M.

A2 - Mantz, R. A.

A2 - Trulove, P. C.

A2 - Ueda, M.

A2 - Carter, M.

A2 - Biddinger, E. J.

A2 - Suroviec, A. H.

A2 - Reichert, M.

A2 - Endres, F.

A2 - Bund, A.

A2 - Ispas, A.

A2 - Fox, D. M.

A2 - De Long, H. C.

PB - Electrochemical Society Inc.

T2 - Symposium on Molten Salts and Ionic Liquids 20 - PRiME 2016/230th ECS Meeting

Y2 - 2 October 2016 through 7 October 2016

ER -

Martens S, Ispas A, Asen L, Seidl L, Stimming U, Schneider O et al. Influence of fluid dynamics on the electrochemical deposition of tantalum. in Haverhals LM, Mantz RA, Trulove PC, Ueda M, Carter M, Biddinger EJ, Suroviec AH, Reichert M, Endres F, Bund A, Ispas A, Fox DM, De Long HC, Hrsg., Molten Salts and Ionic Liquids 20. 15 Aufl. Electrochemical Society Inc. 2016. S. 287-295. (ECS Transactions; 15). doi: 10.1149/07515.0287ecst

Influence of fluid dynamics on the electrochemical deposition of tantalum

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