Improvement of relayed—NOESY type experiments by implantation of spin‐lock sequences

H. Kessler; G. Gemmecker; B. Haase; S. Steuernagel

doi:10.1002/mrc.1260261018

Improvement of relayed—NOESY type experiments by implantation of spin‐lock sequences

H. Kessler, G. Gemmecker, B. Haase, S. Steuernagel

Johann Wolfgang Goethe University

Publikation: Beitrag in Fachzeitschrift › Artikel › Begutachtung

13 Zitate (Scopus)

Abstract

Several Relayed—NOESY type pulse sequences are discussed which use spin‐lock periods for one or both of the two transfer steps. The use of such experiments for the sequence analysis of peptides is shown. The requirements for a successful application of special data processing techniques are explained. Even in conformationally rigid peptides where these conditions are no longer fulfilled, the 2D techniques described represent a sensitive and reliable method for the sequential assignment of the spin systems.

Originalsprache	Englisch
Seiten (von - bis)	919-926
Seitenumfang	8
Fachzeitschrift	Magnetic Resonance in Chemistry
Jahrgang	26
Ausgabenummer	10
DOIs	https://doi.org/10.1002/mrc.1260261018
Publikationsstatus	Veröffentlicht - Okt. 1988
Extern publiziert	Ja

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10.1002/mrc.1260261018

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abstract = "Several Relayed—NOESY type pulse sequences are discussed which use spin‐lock periods for one or both of the two transfer steps. The use of such experiments for the sequence analysis of peptides is shown. The requirements for a successful application of special data processing techniques are explained. Even in conformationally rigid peptides where these conditions are no longer fulfilled, the 2D techniques described represent a sensitive and reliable method for the sequential assignment of the spin systems.",

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author = "H. Kessler and G. Gemmecker and B. Haase and S. Steuernagel",

year = "1988",

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AU - Haase, B.

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AB - Several Relayed—NOESY type pulse sequences are discussed which use spin‐lock periods for one or both of the two transfer steps. The use of such experiments for the sequence analysis of peptides is shown. The requirements for a successful application of special data processing techniques are explained. Even in conformationally rigid peptides where these conditions are no longer fulfilled, the 2D techniques described represent a sensitive and reliable method for the sequential assignment of the spin systems.

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KW - Improved Relayed—NOESEY type pulse sequences

KW - Sequence analysis of peptides

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Improvement of relayed—NOESY type experiments by implantation of spin‐lock sequences

Abstract

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